Инд. авторы: | Darin F.A., Sorokoletov D.S., Rakshun Y.V., Darin A.V., Veksler I.V. |
Заглавие: | On the Search and Localization of Platinum-Group Microelements in Samples of the Chromite Horizon in the Bushveld Complex |
Библ. ссылка: | Darin F.A., Sorokoletov D.S., Rakshun Y.V., Darin A.V., Veksler I.V. On the Search and Localization of Platinum-Group Microelements in Samples of the Chromite Horizon in the Bushveld Complex // Journal of Surface Investigation: X-Ray, Synchrotron and Neutron Techniques. - 2018. - Vol.12. - Iss. 1. - P.123-127. - ISSN 1027-4510. - EISSN 1819-7094. |
Внешние системы: | DOI: 10.1134/S1027451018010263; РИНЦ: 35489905; SCOPUS: 2-s2.0-85045282268; WoS: 000429574100022; |
Реферат: | eng: The search for microinclusions of light platinoids (Ru and Pd) in samples of the Bushveld intrusion complex (South Africa) and corresponding examination are performed by scanning X-ray fluorescence analysis at the SR XRF experimental station with the help of the VEPP-3 storage ring at the Collective-Use Center "Siberian Synchrotron and Terahertz Radiation Center" based at the Budker Institute of Nuclear Physics, Siberian Branch, Russian Academy of Sciences. The samples are prepared as plane parallel ground plates 2 mm in thickness. First, one-dimensional scanning with a wide beam (1 x 20 mm) of monochromatic radiation with an excitation energy of 20 and 30 keV is performed. Then, the region with higher contents of light platinoids is two-dimensionally scanned with a beam (30 x 45 mu m) which is focused with a polycapillary lens. Sample surface mapping enables identification of a few individual particles 50-100 mu m in size with a high Pd content. The potential for micro-XAFS investigation of an individual particle is demonstrated. |
Ключевые слова: | SYNCHROTRON; X-RAY-FLUORESCENCE; platinum-group metals; X-ray fluorescence analysis; synchrotron radiation; polycapillary lens; SCIENCES; |
Издано: | 2018 |
Физ. характеристика: | с.123-127 |
Цитирование: | 1. T. Bultreys, W. De Boever, and V. Cnudde, Earth-Sci. Rev. 155, 93 (2016). 2. G. Qian, Y. Li, and A. Gerson, Surf. Sci. Rep. 70 (1), 86 (2015). 3. I. De La Calle, N. Cabaleiro, V. Romero, I. Lavilla, and C. Bendicho, Spectrochim. Acta, Part B 90, 23 (2013). 4. U. Fittschen and G. Falkenberg, Spectrochim. Acta, Part B 66 (8), 567 (2011). 5. A. V. Dar’in and Ya. V. Rakshun, Nauchn. Vestn. Novosib. Gos. Tekh. Univ., No. 2 (51), 112 (2013). 6. D. S. Sorokoletov, Ya. V. Rakshun, E. P. Voytovich, and F. A. Darin, Phys. Procedia 84, 295 (2016). 7. A. V. Dar’in and Ya. V. Rakshun, Nauchn. Vestn. Novosib. Gos. Tekh. Univ., No. 2 (51), 119 (2013). 8. A. P. Sedunova, I. V. Veksler, and A. V. Dar’in, Geol. Polezn. Iskop. Zapadn. Urala, No. 16, 85 (2016). 9. A. P. Sedunova, I. V. Veksler, V. M. Zhdanov, A. V. Dar’in, K. P. Kazymov, and D. Rid, in Problems on Mineralogy, Petrography, and Metallogeny. Scientific Readings in Memoriam of P. N. Chirvinskii (Perm State Univ., Perm, 2016), Issue 19, p. 302 [in Russian]. 10. I. V. Veksler, D. L. Reid, P. Dulski, J. K. Keiding, M. Schannor, H. Lutz, and R. B. Trumbull, J. Petrol. 56 (6), 1229 (2015). 11. K. Zolotarev, G. Kulipanov, E. Levichev, N. Mezentsev, V. Pindyurin, P. Piminov, and B. Tolochko, Phys. Procedia 84, 4 (2016). 12. P. Piminov, G. Baranov, A. Bogomyagkov, et al., Phys. Procedia 84, 19 (2016). 13. D. S. Sorokoletov, Y. V. Rakshun, and F. A. Dar’in, Optoelectron., Instrum. Data Process. 51 (3), 293 (2015). 14. A. V. Darin, I. V. Veksler, and Ya. V. Rakshun, J. Surf. Invest.: X-ray, Synchrotron Neutron Tech. 10 (1), 88 (2016). 15. S. R. Suttona, M. L. Riversa, S. Bajta, K. Jones, J. V. Smith, Nucl. Instrum. Methods Phys. Res., Sect. A 347, 412 (1994). |