Инд. авторы:	Simonova E.A., Kokh A.E., Kononova N.G., Shevchenko V.S., Kokh D.A., Vlezko V.A., Fedorov P.P.
Заглавие:	Phase equilibria in the ternary reciprocal system Li, Ba//BO2, F and growth of bulk β-BaB2O4 crystals
Библ. ссылка:	Simonova E.A., Kokh A.E., Kononova N.G., Shevchenko V.S., Kokh D.A., Vlezko V.A., Fedorov P.P. Phase equilibria in the ternary reciprocal system Li, Ba//BO2, F and growth of bulk β-BaB2O4 crystals // Journal of Applied Crystallography. - 2017. - Vol.50. - Iss. 1. - P.22-29. - ISSN 0021-8898. - EISSN 1600-5767.
Внешние системы:	DOI: 10.1107/S1600576716017970; РИНЦ: 29477547; SCOPUS: 2-s2.0-85011655959; WoS: 000394289400003;
Реферат:	eng: In order to find the optimum solvent for the growth of nonlinear optical β-BaB2O4 crystals, the phase relationships in the ternary reciprocal system Li, Ba//BO2, F have been studied using solid state synthesis, differential thermal analysis and X-ray powder diffraction. Isothermal and polythermal sections of the system Li, Ba//BO2, F are reported. In the studied system, the following compounds are formed: LiBa2B5O10 (melts by peritectic reaction at 930°C, i.e. 1203 K) and LiBaF3 (melts incongruently at 850°C, i.e. 1123 K). Visual polythermal analysis of seeding and growth of β-BaB2O4 crystals in this system was carried out. The primary crystallization field of β-BaB2O4 was defined. Using the top-seeded pulling technique, a β-BaB2O4 crystal of 93 mm in diameter, 34 mm in height and 520 g in weight has been grown. © 2017 International Union of Crystallography.
Ключевые слова:	Peritectic reaction; Nonlinear optics; Borates; Ternary reciprocal systems; Solid-state synthesis; Primary crystallization fields; Polythermal sections; Phase relationships; Non-linear optical material; borates; X ray powder diffraction; Thermoanalysis; Single crystals; Phase equilibria; Phase diagrams; Optical materials; Lithium; Differential thermal analysis; Single-Crystal growth; Phase diagrams; nonlinear optical materials; borates;
Издано:	2017
Физ. характеристика:	с.22-29
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