Инд. авторы:	Hu M.-Y., Fan X.-T., Stoll B., Kuzmin D.V., Liu Y., Liu Y., Sun W., Wang G., Zhan X.-C., Jochum K.P.
Заглавие:	Preliminary Characterisation of New Reference Materials for Microanalysis: Chinese Geological Standard Glasses CGSG-1, CGSG-2, CGSG-4 and CGSG-5
Библ. ссылка:	Hu M.-Y., Fan X.-T., Stoll B., Kuzmin D.V., Liu Y., Liu Y., Sun W., Wang G., Zhan X.-C., Jochum K.P. Preliminary Characterisation of New Reference Materials for Microanalysis: Chinese Geological Standard Glasses CGSG-1, CGSG-2, CGSG-4 and CGSG-5 // Geostandards and Geoanalytical Research. - 2011. - Vol.35. - Iss. 2. - P.235-251. - ISSN 1639-4488. - EISSN 1751-908X.
Внешние системы:	DOI: 10.1111/j.1751-908X.2010.00097.x; SCOPUS: 2-s2.0-79956137227;
Реферат:	eng: Four silicate glasses were prepared by the fusion of about 1kg powder each of a basalt, syenite, soil and andesite to provide reference materials of natural composition for microanalytical work. These glasses are referred to as 'Chinese Geological Standard Glasses' (CGSG) -1, -2, -4 and -5. Micro and bulk analyses indicated that the glasses are well homogenised with respect to major and trace elements. Some siderophile/chalcophile elements (e.g., Sn, Pt, Pb) may be heterogeneously distributed in CGSG-5. This paper provides the first analytical data for the CGSG reference glasses using a variety of analytical techniques (wet chemistry, XRF, EPMA, ICP-AES, ICP-MS, LA-ICP-MS) performed in nine laboratories. Most data agree within uncertainty limits of the analytical techniques used. Discrepancies in the data for some siderophile/chalcophile elements exist, mainly because of possible heterogeneities of these elements in the glasses and/or analytical problems. From the analytical data, preliminary reference and information values for fifty-five elements were calculated. The analytical uncertainties [2 relative standard error (RSE)] were estimated to be between about 1% and 20%. © 2010 The Authors. Geostandards and Geoanalytical Research © 2010 International Association of Geoanalysts.
Ключевые слова:	Glass; Uncertainty analysis; Trace elements; Tin; Standards; Silicates; Platinum; Mass spectrometers; Lead; Chemical analysis; Atomic emission spectroscopy; Trace element composition; Reference values; Reference glasses; MPI-DING; Major element composition; Homogeneity; CGSG-1; -5; Trace element composition; Reference values; Reference glasses; MPI-DING; Major element composition; Homogeneity; CGSG-1; -5;
Издано:	2011
Физ. характеристика:	с.235-251