Инд. авторы: | Lavrent'ev Yu.G., Romanenko I.M., Novikov M.P., Usova L.V., Korolyuk V.N. |
Заглавие: | Synthetic TRPO4 crystals as reference samples in the quantitative X-ray electron probe microanalysis of rare-earth elements |
Библ. ссылка: | Lavrent'ev Yu.G., Romanenko I.M., Novikov M.P., Usova L.V., Korolyuk V.N. Synthetic TRPO4 crystals as reference samples in the quantitative X-ray electron probe microanalysis of rare-earth elements // Journal of Analytical Chemistry. - 2011. - Vol.66. - Iss. 9. - P.831-837. - ISSN 1061-9348. - EISSN 1608-3199. |
Внешние системы: | DOI: 10.1134/S1061934811090085; SCOPUS: 2-s2.0-80053992237; |
Реферат: | eng: Crystals of 15 rare-earth element phosphates, which provide a set of standard reference samples in X-ray electron probe microanalysis, were synthesized and tested for homogeneity and stoichiometry. The phosphates were synthesized in two stages, the preparation of aqueous phosphates and crystal growth in a solution of potassium polymolybdate K2Mo 3O10. The tests of the synthesized crystals confirmed their reliability as reference samples. © 2011 Pleiades Publishing, Ltd.
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Ключевые слова: | X rays; Stoichiometry; Probes; Potassium; Phosphates; Heterojunctions; Electron probe microanalysis; Crystals; Crystal growth; Carrier concentration; Two stage; Synthetic crystals; reference samples; Rare-earth phosphates; Electron probe; X-ray electron probe microanalysis; synthetic crystals; reference samples; rare-earth phosphates; Corrosion resistance; |
Издано: | 2011 |
Физ. характеристика: | с.831-837 |